Determination of polycyclic aromatic hydrocarbons in tea infusions samples by high performance liquid chromatography with fluorimetric detection

01 Pubblicazione su rivista
Girelli Anna Maria, Apriceno Azzurra, Tarola Anna Maria, Francesca Tortora And
ISSN: 1745-4557

This study focuses on the contamination of 15 polycyclic aromatic hydrocarbons (PAHs) ,
recommended by the US Environmental Protection Agency, in 10 tea brands distributed in Italy.
Analysis were carried out with a procedure based on saponification, liquid-liquid extraction and
PAHs determination by high performance liquid chromatography with fluorescence detector. A
comparison with ultrasonic extraction in bath water was also reported. Contamination is expressed
as the sum of analyzed PAHs and ranged between 347 and 4120 ng/l with a mean value of 1675
ng/l. PAHs with 3-4 rings were dominant with a contribution of 92% , while 7% and 1% were
found for PAHs with 5 and 6 rings, respectively. Moreover, data revealed that three samples
exceeded the EU 2008 criteria established for drinking water in which the sum of
benzo[k]fluoranthene, benzo[b]fluoranthene, benzo[g,h,i]perylene and indeno[1,2,3-cd]pyrene is
considered (<100 ng/L) and two samples exceeded the 10 ng/L level allowed for benzo[a]pyrene

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