The group has more than twentyfive years of experience in the field of organic electrochemistry, particularly for the synthesis of materials for organic electronics, small molecules of industrial and pharmaceutical interest, incorporation of carbon dioxide in organic compounds. The research group has specific skills in organic synthesis, electrochemical characterization of organic molecules and salts, also in view of their application in organic electronics. In the laboratory various instruments are available for basic and applied electrochemical studies, for preparation and for some spectroscopic characterizations of the materials. The group has always carried out training of young researchers in the field of organic and electroorganic synthesis. Aims of the work are: Chemical syntheses, characterization and electrochemical studies of new organic compounds and nanocomposite materials used in photovoltaics, OLEDs, plastic scintillators, erbium infrared emitters, photodetectors, semiconductors for sensor applications, and more. To study organic and redox reactions by electrochemical techniques, in particular to carry out the electrochemical synthesis of fine chemicals and of products of interest for pharmaceutical and chemical industry. Development of electrochemical syntheses in ionic liquids as greener solvents than VOCs. HPLC-PDA-MS/MS analysis provides information on the chemical composition of different matrices of interest, as the products mixture resulting from organic reactions, or real matrices from food and beverages industry, paying particular attention to the antioxidant phenolic components for nutritional and waste recovery purposes, to name a few.
Laboratory of Electrochemistry, Organic Synthesis & Mass Spectrometry (LEOS-MS)
Descrizione
Tipologia
Chimico, Nanotecnologico, Strumentale
Attività
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Responsabile
Nome | Struttura | |
Leonardo Mattiello | leonardo.mattiello@uniroma1.it | DIPARTIMENTO DI SCIENZE DI BASE ED APPLICATE PER L'INGEGNERIA |
ERC scientific sector
PE4_2, PE4_5, PE4_8, PE5_5, PE5_6, PE5_7, PE5_17, LS9_5
Dipartimento o centro ospitante
Personale docente e di ricerca
KET
Nanotechnologies, Advanced materials
Strumenti e attrezzature
Nome | Descrizione | Servizi Offerti | Tipologia |
AMEL System 5000 Multifunctional Electrochemical System | Electrochemistry apparatus | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
AMEL Multifunctional Electrochemical System | Electrochemistry apparatus | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
BioChromato Smart Evaporator System | Distillation apparatus | Strumenti da laboratorio (agitatori, piastre riscaldanti, centrifughe, autoclavi, ecc) | |
Jouan LP3 Freeze Dryer apparatus | Freeze Dryer apparatus | Strumenti da laboratorio (agitatori, piastre riscaldanti, centrifughe, autoclavi, ecc) | |
Analytical Chemistry Lab (Glove Box) | Glove Box | Strumenti da laboratorio (agitatori, piastre riscaldanti, centrifughe, autoclavi, ecc) | |
Shimadzu HPLC System | HPLC System | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
Hewlett-Packard GC-MS Gas Chromatograph/Mass Spectrometer Apparatus | Gas Chromatograph/Mass Spectrometer Apparatus | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
Waters HPLC-PDA-MS/MS Liquid Chromatography/Tandem Mass Spectrometry system | Liquid Chromatography/Tandem Mass Spectrometry system | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
UV-Vis Spectroelectrochemistry ChemStation | SpectroElectrochemistry apparatus | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
Magritek Spinsolve 60 MHz Benchtop NMR Spectrometer | Nuclear Magnetic Resonance apparatus | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) | |
Nuclear Magnetic Resonance apparatus | InfraRed Spectrometer | Attrezzature principali per la ricerca (piccole/medie/grandi attrezzature) |
Responsabile tecnico
Nome | Struttura | |
Marco Di Pilato | marco.dipilato@uniroma1.it | DIPARTIMENTO DI SCIENZE DI BASE ED APPLICATE PER L'INGEGNERIA |